Friday, December 19, 2025

Michael R. Notis et al., on the Use of Steel in the Iron Age I era (1200-1000 BC)

The following excerpts come from:

 

Michael R. Notis, Vincent C. Pigott, Patrick E. McGovern, K.H. Liu, and C.P. Swann. “The Metallurgical Technology: The Archaeometallurgy of the Iron IA Steel,” in The Late Bronze and Early Iron Ages of Central Transjordan: The Baq’ah Valley Project, 1977–1981, ed. Patrick E. McGovern (University Museum Monograph 65; Philadelphia: University Museum, 1986), 272–278.


 

Among the most significant finds in Cave A4 was a group of eleven complete pieces of iron jewelry— eight anklets or bracelets and three rings—and forty fragments, dating to Iron IA. Three basic types of anklet/bracelets are represented: (1) with terminals open, (2) with ends overlapping and superimposed one above the other, and (3) with ends overlapping side-by-side (see Ch. 7). Two types of rings can be distinguished, each with a rectangular cross-section, but one had open ends, the other overlapping ends. Waldbaum (1978) in her survey ofi ron artifacts recovered from excavations in the eastern Mediterranean lists five objects from two LB II Palestinian contexts, and about twenty more from various twelfth century B.C. loci at seven Palestinian sites. The East Bank of the Jordan is represented only by a pair of bracelets and pair of rings from a transitional LB/early Iron Age tomb at Madaba (Harding 1953). They comprise one example each of an open-ended and an overlapping, superimposed type, as defined above.

 

To these examples must now be added an iron (steel) blade from Tomb 4 in the East Cemetery at Pella, dated to the Middle Bronze Age (Smith et al. 1984), an unidentified fragment from an LB II tomb on Jebel al-Nuzha near Amman (Dajani 1966c), part of a totally corroded anklet or bracelet from the LB II Cave B3 (Ch. 7), and an early Iron Age knife from Tomb 113 at Tell es-Sa‘idiyeh (Pritchard 1980: 20, fig.) 15.6).

 

With the excavation of Cave A4, the number of iron artifacts from twelfth century B.C. Palestine has approximately tripled, while for Transjordan it has been increased almost sevenfold. These figures rep-resent a major statistical shift in the distribution of iron artifacts in the Eastern Mediterranean. The Transjordanian plateau is clearly of great importance in understanding the development and early history of iron (steel) metallurgy. (p. 272)

 

Table from p. 273 (click to enlarge):

 



 

 

Anklet or Bracelet (A4.55; Fig. 84.13, Pl. 29c)

 

The extent and inhomogeneity of carburization of the metal in this artifact are illustrated in Pl. 48a. The microstructure of A4.55 is extremely variable; overall it corresponds to that of a hypoeutectoid steel, but there are regions with typically hypereutectoid features. In addition, there are precipitated phase(s) of broadly varying size in the proeutectoid ferrite and in the ferritic component region of the pearlite (PI. 48b). To simplify the discussion, the nature of the precipitated phases will be discussed after the other microstructural features have been elucidated.

 

The morphological features of proeutectoid ferrite and proeutectoid cementite have been classified into several main categories: idiomorphic, allotriomorphic, and Widmanstatten (Dube et al. 1958); further subdivisions have also been introduced within each main category (Aaronson 1962). The composition temperature range for the formation of each of the three main types of proeutectoid structural components are described in these references; the different morphological features of the proeutectoid phases in a given alloy may correspond to different undercooling conditions through which the transformation has taken place. Thus, for a hypoeutectoid steel, the idiomorphic ferrite forms with slight undercooling, and the allotriomorphic ferrite and then the Widmanstatten ferrite form with increasing degrees of undercooling in a given alloy (1.e., for a given carbon content). A similar sequence 1s proposed for the formation of proeutectoid cementite in hypereutectoid steels. The degree of undercooling required for a specific morphological feature is also influenced by the austenite grain size, with larger grain size extending the range of formation of the Widmanstatten morphology. A steel with larger grain size has a greater tendency to form a Widmanstatten structure, which is why Widmanstatten ferrite is frequently observed in the microstructure of cast steel, or in overheated hot-worked steels after normalizing treatments.  (p. 273)

 

 

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